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CILAS laser particle size distribution
CILAS laser - the automated auto sampler

MODELS \ range of measure
(direct access)

990 \ 0.2 – 500 µm
1090 \ 0.04 – 500 µm
1190 \ 0.04 – 2500 µm
Size Expert
Accessories :
- video camera,
- autosampler,
- alcohol regenerator,
- small volume unit.

ISO 13320
21 CFR-11

FRAUNHOFER / MIE
Reference powders



 

FRAUNHOFER THEORY


Assumptions
Spherical, non-porous and opaque particles,
Diameter d > wavelength l,
Particles are distant enough from each other,
Random motion,
All the particles diffract the light with the same efficiency, regardless of.

Characteristic of the Airy shape

Characteristic of the Airy shape : 3d graph
Characteristic of the Airy shape : 2d graph

Circular,
Consisting in concentric rings I = f (a),
Spacing and size of the rings are linked to the particle size,
The fist zero angle is related to the diameter d by 1.22 l/d,
75% of the total energy is concentrated in the first lobe.

 

Principle

Principle

 

Aspect of the diffraction pattern with respect to the particle size

System
System
for a large particle
System
System
for a small particle

The observation of the diffraction pattern at finite distance is done through a lens (L) placed between the laser source and the detector

The observation of the diffraction pattern at finite distance

The diffraction patterns of particles having the same size converge at the same point whatever them location with respect to the lens,
The first zero on the detector is 1.22 lf/d where f is the focal length.


MIE THEORY

The Fraunhofer theory is applicable for large particles compared to the wavelength l (diffusion and absorption are not considered). 
For smaller particles, it is appropriate to use Mie Theory.
Mie schema
The Mie model takes into account both diffraction and diffusion of the light around the particle in its medium. 
To use the Mie model, it is necessary to know the complex refractive index of both the sample and the medium. 
This complex index has a real part, which is the standard refractive index, and an imaginary part, which represents absorption.

Complex index = m
m = a + b
a : real part
b : imaginary part

Because of the importance of this model, CILAS has crated a fast algorithm, which enables the user to get, within seconds, diffusion results using Mie theory and taking into account the complex index of the sample.

 
What’s New
 

sharpe analysing

Come and see our solutions at the following trade shows : (for more details, click on the shows).

USA ............................
optical Pittcon 2012
Booth 2635
Orlando - USA
11 - 15 March
www.pittcon.org/

opticalParticle Society of Minnesota Show
Roseville - USA
March

optical ACeRS Regional Refractories Show
St Louis - USA
28 March

optical Chicago Catalyst Show
Chicago - USA
May

optical Powder and Bulk Solids
Booth 2738
Rosemont - USA
8 - 10 May

optical Southeast Catalyst Show
Asheville - USA
September

optical MS & T 2012
Booth F7
Pittsburgh - USA
October

optical American Association of Pharmaceutical Scientists
Chicago - USA
14 - 18 October

EUROPE ......................
optical Analytica 2012
Booth A2-532
Munich - GERMANY
17 to 20 April
www.analytica.de/en/Home

optical 11th World Filtration Congress
Booth F7
Graz - AUSTRIA
16 to 20 April

optical Achema 2012
Booth 4.2 J50
Frankfurt - GERMANY
18 to 22 June
www.achema.de/index.php?
selectedArea=1&selectedItem=1&spkz

ASIA ..........................
optical ArabLab 2012
Dubai - UAE
26 - 29 March
www.arablab.com

particle sharpe
granulometre